Rota

Posted by RC Mishra | 2:26 AM | 0 comments »

Vapor
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I found this fascinating quote today:



Are you not feeling comfortable with inplace editing facility of OLE objects embedded in Word/PowerPoint documents?All Info About Chemistry, Aug 2008



You should read the whole article.


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I found this fascinating quote today:



Select the whole drawing or the part you feel needs to be adjusted for bond angle and length’s and click on the Cleanup structure button on the tool bar.All Info About Chemistry, Aug 2008



You should read the whole article.


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Leonid HurwiczThe Nobel Prize in Chemistry for 2007 was awarded to Gerhard Ertl (Germany, 1936) "for his studies of chemical processes on solid surfaces". This science is important for the chemical industry and can help us to understand such varied processes as why iron rusts, how fuel cells function and how the catalysts in our cars work.

External link Gerhard Ertl - Fritz-Haber-Institut der Max-Planck-Gesellschaft, Berlin, Germany.

Gerhard Ertl is a member of the Advisory Editorial Board for Elsevier's Chemical Physics Letters and formerly a handling editor for both Surface Science and Surface Science Reports.

In recognition of the importance of his work, Elsevier is pleased to offer open access to key articles that Gerhard Ertl has published with them.

Polynuclear metal carbonyl compounds and chemisorption of CO on transition metal surfaces
Chemical Physics Letters
Volume 42, Issue 1, 15 August 1976, Pages 115-118
H. Conrad, Gerhard Ertl, H. Knözinger, J. Küppers and E. E. Latta

The role of potassium in the catalytic synthesis of ammoniaChemical Physics Letters
Volume 60, Issue 3, 15 January 1979, Pages 391-394
Gerhard Ertl, M. Weiss and S. B. Lee

Adsorption and thermal decomposition of ammonia on a Ni(110) surface - isolation and identification of adsorbed NH2 and NH
Surface Science
Volume 175, Issue 11, 1986
Bassignana, Wagemann, Kuppers and Gerhard Ertl

Adsorption of hydrogen on a Pt(111) surface
Surface Science
Volume 54, Issue 2, 1976
Christmann, Gerhard Ertl and Pignet

 

Leonid Hurwicz
Gerhard Ertl
Fritz-Haber-Institut der Max-Planck-Gesellschaft, Berlin, Germany

Video
View a video clip of the Nobel Prize Award Ceremony

Research

Posted by RC Mishra | 9:26 PM | | 0 comments »

Doctoral

Thesis title:

'Synthetic Studies in Carbohydrate Molecular Diversity: Development of Anti-parasitic Agents'

Guide/Supervisor:

Dr Rama Pati Tripathi Scientist E-II

Central Drug Research Institute (CSIR)

Lucknow-226001, INDIA

Post Doctoral

Project 1: January 2005-February 2006

Title :Metodologie Syntetiche per la preparazione di composti a potenziale inetresse tossicologico, in particolare nucleosidi e nucleotidi

[Synthetic methods for the preparation of the compounds of toxicological interest, in particular nucleosides and nucleotides]

Guide/Supervisor: Prof (Dr) Gloria Cristalli, Deputy Vice Chancellor, University of Camerino, Camerino, (MC) 62032. Italy

Project 2: March 2006-June 2007

Title:Carattarizzazione analitica di prodotti tipici dell’ Appennino marchegiano e sintesi di molecule caratterizzanti

[Analytical characterization of the products of the typical of the Marche region and the synthesis of the characterized molecules]

Guide/Supervisor: Prof. (Dr.) Gloria Cristalli, Deputy Vice Chancellor & Prof. (Dr.) Gabriella Marucci, Department of Chemistry, University of Camerino, Camerino, (MC) 62032. Italy

Project 3: July 2007-Till date

Title:Sintesi e caratterizzazione di nuovi nucleosidi e nucleotidi purinici

[Synthesis and characterization of new purine nucleosides & nucleotides]

Guide/Supervisor: Prof. (Dr.) Gloria Cristalli, Deputy Vice Chancellor, Department of Chemistry, University of Camerino, Camerino, (MC) 62032. Italy

Thesis Front Page

Posted by RC Mishra | 8:38 PM | 0 comments »

SYNTHETIC STUDIES IN CARBOHYDRATE MOLECULAR DIVERSITY: DEVELOPMENT OF ANTIPARASITIC AGENTS

THESIS SUBMITTED

TO

Dr. R. M. L., AVADH UNIVERSITY

clip_image002[4]

FAIZABAD

FOR THE DEGREE OF

DOCTOR OF PHILOSOPHY

IN

CHEMISTRY

By

Ram Chandra Mishra

M. Sc. (Chemistry)

MEDICINAL & PROCESS CHEMISTRY DIVISION

CENTRAL DRUG RESEARCH INSTITUTE

(Council of Scientific and Industrial Research)

Lucknow-226001, INDIA

2004

The Dragendorff Reagent

Posted by RC Mishra | 8:09 PM | 1 comments »

Dragendorff Reagent:

The Dragendorff's Reagent is used for the detection of Nitrogenous compounds, alkaloids, antiarrhythmic drugs and surfactants and is also good detector for Phenols.

There are two kinds for preparations, each procedure says preparation of Solution A and Solution B, both are then mixed to use.

1st Method:

Solution A: 1.7 g basic bismuth nitrate in 100 ml water/acetic acid (4:1).

Solution B: 40.0 g potassium iodide in 100 ml of water.

Mix reagents together as follows: 5 ml A + 5 ml B + 20 ml acetic acid + 70 ml water.

Spray plates, orange spots develop. Spots intensify if sprayed later with HCl, or 50% water-phosphoric acid. Good for phenols.

 

2nd Method:


Solution A: 1.7 g basic bismuth nitrate and 20 g tartaric acid in 80 ml of water. 
Solution B:  16 g potassium iodide in 40 ml of water.

Stock solution: (stable several weaks in a refrigerator): mix equal volumes of solutions A and B

 
Procedure:  Spray with a solution of 10 g tartaric acid, 50 ml water & and 5 ml stock solution.